Contents: PART I: DETERMINATION OF MOLECULAR WEIGHT • Experiment 1: Rast’s Method • Experiment 2: Beckmann Method • Experiment 3: Viscosity Measurements • Experiment 4: Steam Distillation • PART II: THERMODYNAMIC PROPERTIES OF SOLUTION • Experiment 5: Solubility of Naphthalene in Benzene • Experiment 6: Partition Coefficient for the Distribution of Iodine between Water and Carbon tetrachloride • Experiment 7: Equilibrium Constant for Homogeneous Equilibria and Determining the Concentration of a given Solution • Experiment 8: Association Factor of Benzoic Acid • Experiment 9: Molecular Formula of Copper-ammonia Complex by the Partition Coefficient Method • PART III: THERMOCHEMICAL EXPERIMENTS • Experiment 10: Heat of Solution of Oxalic Acid front Solubility Measurements • Experiment 11: Heat of Neutralisation of a Strong Acid by a Strong Base • Experiment 12: Vapour Pressure and Enthalpy of Vapourisation of Water • PART IV: PHASE EQUILIBRIA • Experiment 13: Transition Temperature of a Salt Hydrate • Experiment 14: Critical Solution Temperature of Partially Miscible Liquid System • Experiment 15: Effect of Electrolytes on the Critical Solution Temperature • Experiment 16: Temperature-Composition Diagram for Two Component Liquid Azeotropic Systems • Experiment 17: Two Component Simple Eutectic Systems • Experiment 18: Two Component-Compound Forming Systems • Experiment 19: Three Component Liquid Systems: Acetic Acid—Benzene—Water • PART V: CHEMICAL KINETICS • Experiment 20: Acid-Catalysed Hydrolysis of Methyl Acetate • Experiment 21: Alkaline Hydrolysis of Ethylacetate Volumetry • Experiment 22: Alkaline Hydrolysis of Ethylacetate by Conductometry • Experiment 23: Activation Energy for the Acid—Catalysed Hydrolysis of Methylacetate • Experiment 24: Dissociation of Trichloroacetic Acid—Kinetic Method • Experiment 25: Hydrolysis of t-amyl iodide • Experiment 26: Determination of Order for the Peroxide—Iodide Reaction • Experiment 27: Determination of Order for the Persuiphate—lodide Reaction • Experiment 28: Kinetics of lodination of Acetone by Spectrophotometry • Experiment 29: Evaluation of First Order Rate Constant Potentiometry • Experiment 30: Kinetics of a Polymerization Reaction • Experiment 31: Kinetics of Catalytic Decomposition of Hydrogen Peroxide • Experiment 32: Thermal Decomposition of Potassium Chlorate • Experiment 33: Effect of Surface Area of Catalyst and Temperature on the Kinetics of Metal-Acid Reaction • Experiment 34: Catalytic Constant of an Acid • Experiment 35: Mechanism of the Oxidation of an Organic Compound from Kinetic Data • Experiment 36: Rate Constant for the Decomposition of Hydrogen Peroxide Over Platinum • Experiment 37: Polymerisation of methylmethacrylate Experiment 38: Light Intensity (in Einstein/minute) Emitted by a Source—Actinometry • Experiment 39: Inversion of Sucrose—Polarimetry • Experiment 40: Decomposition of Diacetone Alcohol Using Dilatometer • Experiment 41: Rate of Decomposition of Ammonium Nitrite (or Benzene Diazonium Chloride) • Experiment 42: Evaluation of Rate Constant by Guggenheim Method • Experiment 43: Effect of Ionic Strength on the Rate of Persulphate — Iodide Reaction • Experiment 44: Kinetics of Oxidation of Alcohol by Potassium Dichromate—Spectrophotometry • PART VI: SURFACE CHEMISTRY • Experiment 45: Adsorption Characteristics of Acetic Acid on Charcoal • Experiment 46: Surface Tension of a Liquid Using Stalagmometer • Experiment 47: Critical Micelle Concentration from Surface Tension Measurements • PART VII: PHOTOMETRY • Experiment 48: Verification of Beer and Lamberfs Law • Experiment 49: Jobts Continuous Variation Method • Experiment 50: Simultaneous Estimation of Manganese and Chromium in a Solution of Dichromate and Permanganate Mixture • Experiment 51: Spectrophotometric Determination of Critical Micelie Concentration • PART VIII: CONDUCTOMETRY • Experiment 52: Determination of Cell Constant • Experiment 53: Verification of Onsager’s Equation and Determination of Equivalent Conductance at Infinite Dilution of Strong Electrolytes • Experiment 54: Verification of Ostwalds Dilution Law and Determination of Dissociation Constant of Weak Acids • Experiment 55: Verification of Walden’s Rule • Experiment 56: Conductometric Determination of Critical Micelle Concentration • Experiment 57: Titration of a Strong Acid with a Strong Base • Experiment 58: Titration of a Weak cid with a Strong Base • Experiment 59: Titration of a Mixture of Strong and Weak Acid with a Strong Base • Experiment 60: Precipitation Titration and Determination of Solubility of a Sparingly Soluble Salt • PART IX: POTENTIOMETRY • Experiment 61: Transport Numbers of Silver and Nitrate Ions by l-Iittorf’s Method • Experiment 62: Standard Electrode Potential of Cu and Ag Electrodes and Determination of the Potential Difference in a Concentration Cell • Experiment 63: Thermodynamic Parameters of a Reaction from EMF Measurement • Experiment 64: Formal Potential of a Redox Couple • Experiment 65: p1-I of a Buffer Solution • Experiment 66: Solubility Product and the Instability Constant • Experiment 67: Activity of Hydrogen Ions Using the Hydrogen Electrode • Experiment 68: Hydrolysis Constant and the Degree of Hydrolysis • Experiment 69: Titration of a Strong/Weak Acid With a Strong Base • Experiment 70: Titration of a Strong and Weak Acid Mixture with a Strong Base • Experiment 71: Dissociation of a Weak Acid by Potentiornetric Titration • Experiment 72: Redox Titration • Experiment 73: Composition of Zinc Ferrocyanide Complex by Potentiometric Titration • Experiment 74: Precipitation Titration of a Mixture of Chloride and Iodide Ions with Silver Nitrate • PART X: ELECTRODE PROCESSES • Experiment 75: Percentage Purity of Copper Sulphate—Electrogravimetry • Experiment 76: Decomposition Potential • Experiment 77: Polarisation Phenomenon • PART XI: VOLTAMETRY • Experiment 78: Reversibility of an Electrochemical Reaction and Determination of Concentration of a given Reducible lon—Polarography • Experiment 79: Formula and the Stability Constant of a Complex by Polarography • Experiment 80: Reversibility of a Redox Process and Determination of the Concentration of a given Solution—Cyclic Voltametry • PART XII: MISCELLANEOUS EXPERIMENTS • Experiment 81: Magnetic Susceptibility by Guoy Balance • Experiment 82: Transition Temperature and Heat of Transition by Differential Thermal Analysis • Experiment 83: Polymorphic Transformation of Solids—Dilatometry • Experiment 84: Electrochemical Nature of Corrosion and its Control • Experiment 85: Current—Voltage Characteristics of a p-n Junction Rectifier • Experiment 86: Dielectric Behaviour of Ceramics by Pse Transion • Experiment 87: Partial Molar Volume of Ethanol—Water Mixture • Experiment 88: Velocity of Sound in Liquids—Ultrasonic Interferometry • Experiment 89: Determination of Very Low Concentration of Metals in Solution by Flame Photometry • Experiment 90: Specific and Molar Refraction of a Liquid by Refractometry • Experiment 91: Dipole Moment ofhiquid • Experiment 92: Estimation of Avogadro Number • Experiment 93: Crystal Structure Determination—X-ray Diffractogram • Experiment 94: Surface Area Determination • Experiment 95: Excited State Propeperties of Molecules • Experiment 96: UV—Visible Spectroscopy • Experiment 97: Infrared Spectroscopy • Experiment 98: Electron Spin Resonance Spectroscopy • Experiment 99: Nuclear Magnetic Resonance Spectroscopy • Experiment 100: Molecular Modeling